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SSH EN 16206:2012

Artikuj ushqimorë - Përcaktimi i arsenikut me spektrometri te absorbimit atomik me gjenerim avujsh hidrure pas tretjes me mikrovalë nen presion (Tretje me acid nitrik 65% dhe peroksid hidrogjeni 30% )

Animal feeding stuffs - Determination of arsenic by hydride generation atomic absorption spectrometry (HGAAS) after microwave pressure digestion (digestion with 65 % nitric acid and 30 % hydrogen peroxide)
27 qer 2013

General information

60.60     16 jan 2013

DPS

DPS/KT 275

European Norm

65.120  

anglisht  

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Scope

This European Standard specifies a method for the determination of total arsenic in animal feeding stuffs by hydride generation atomic absorption spectrometry (HGAAS) after microwave pressure digestion. The limit of quantification is 0,5 µg/l of the test solution. Using a test portion of 0,5 g, a volume of the test solution of 25 ml and an aliquot of 5 ml for pre-reduction the limit of quantification is 0,125 mg/kg in the feed material.
NOTE For feed materials containing organic arsenic species from compounds of marine origin (i.e. arsenobetaine and tetramethylarsine oxide) a higher digestion temperature of the microwave system up to 300 °C may be necessary in order to enable the hydridisation of these arsenic compounds and in order to determine all different kinds of arsenic species in the corresponding feeding stuffs. Alternatively, the digestion procedure of Annex D can be used if the microwave system does not reach higher temperatures up to 300 °C to ensure complete mineralization for HGAAS determination.

Related directives

Directives related to this standards.

70/373/EC

Direktiva e Këshillit 70/373/EEC e 20 korrik 1970 në futjen e metodave të Komunitetit të marrjes së mostrës dhe analizave për kontrollin zyrtar të ushqimit për kafshë

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PUBLISHED
SSH EN 16206:2012
60.60 Standard published
16 jan 2013

Related project

Adopted from EN 16206:2012

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