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Drejtoria e Përgjithshme e Standardizimit
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ISO 18363-3:2017

Animal and vegetable fats and oils — Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS — Part 3: Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol

Dec 7, 2017
95.99 Withdrawal of Standard   Jul 1, 2024

General information

95.99     Jul 1, 2024

ISO

ISO/TC 34/SC 11

International Standard

67.200.10  

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Scope

ISO 18363-3:2017 specifies a procedure for the simultaneous determination of 2-MCPD esters (bound 2-MCPD), 3‐MCPD esters (bound 3‐MCPD) and glycidyl esters (bound glycidol) in a single assay, based on acid catalysed ester cleavage and derivatization of cleaved (free) analytes with phenylboronic acid (PBA) prior to GC/MS analysis.
ISO 18363-3:2017 is applicable to solid and liquid fats and oils. For all three analytes the limit of quantification (LOQ) is 0,1 mg/kg and the limit of detection (LOD) is 0,03 mg/kg.

Life cycle

NOW

WITHDRAWN
ISO 18363-3:2017
95.99 Withdrawal of Standard
Jul 1, 2024

REVISED BY

PUBLISHED
ISO 18363-3:2024

National adoptions

Animal and vegetable fats and oils — Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS — Part 3: Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol

60.60 Standard published

DPS/KT 307 more