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SSH EN 16924:2017

Foodstuffs - Determination of zearalenone in edible vegetable oils by LC-FLD or LC-MS/MS

Sep 28, 2017

General information

60.60     Aug 8, 2017

DPS

DPS/KT 275

European Norm

67.200.10  

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Scope

This European Standard describes a procedure for the determination of the zearalenone content in edible vegetable oils specifically maize germ oil by either of the following techniques: High performance liquid chromatography with fluorescence detection (LC-FLD) or high performance liquid chromatography with tandem mass spectrometry (LC-MS/MS) after basic extraction of the diluted oil.
The method has been validated for zearalenone in naturally contaminated maize germ oil at levels of 61,2 µg/kg to 515 µg/kg [5].
Laboratory experiences [6] have shown that this method is also applicable to other vegetable oils such as wheat germ oil (n = 4), sunflower oil (n = 5), pumpkin seed oil (n = 1), soybean oil (n = 5), hemp seed oil (n = 5), rape seed oil (n = 11), and mixed oils including maize germ oil (n = 3). However occasionally, samples can result in interferences in the FLD-chromatograms. In this case, the detection with MS/MS is recommended.

Related directives

Directives related to this standards.

882/2004

Regulation (EC) No 882/2004 of the European Parliament and of the Council of 29 April 2004 onofficial controls performed to ensure the verification of compliance with feed and food law, animal health and animal welfare rules

Life cycle

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PUBLISHED
SSH EN 16924:2017
60.60 Standard published
Aug 8, 2017

Related project

Adopted from EN 16924:2017

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